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Reaction of 2,3,3-trimethyl-3H-indolium salts with crotonaldehyde

✍ Scribed by A. A. Shachkus; Yu. A. Degutis

Publisher
Springer US
Year
1990
Tongue
English
Weight
232 KB
Volume
26
Category
Article
ISSN
0009-3122

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✍ A. A. Shachkus; R. Yu. Dyagutite; Z. A. Stumbryavichyute πŸ“‚ Article πŸ“… 1990 πŸ› Springer US 🌐 English βš– 284 KB

. A mixture of aldehyde V (1o08 g, 0.005 mole), sodium hydroxide (8 g, 0.2 mole), and benzyl cyanide (0.59 g, 0.005 mole) was refluxed in methanol (80 ml) for 3 h. The solvent was evaporated in vacuo, the residue treated with water, and the solid filtered, washed with water to neutrality, and dried.