Reaction Engineering for Consecutive Enzymatic Reactions in Peptide Synthesis: Application to the Synthesis of a Pentapeptide
✍ Scribed by Salvador Ruiz; Josep A. Feliu; Glòria Caminal; Gregorio Álvaro; Josep López-Santín
- Book ID
- 109388007
- Publisher
- American Institute of Chemical Engineers
- Year
- 1997
- Tongue
- English
- Weight
- 137 KB
- Volume
- 13
- Category
- Article
- ISSN
- 8756-7938
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Raoeived In Japan 25 Deoembu 1971; reoeived in IX for ~bliostian 31 Doeember 1971) We found that the N-phosphonium salt 1) of pyridine(1) was formed via.the oxidation of phosphorous acid and its esters with mercuric chloride in pyridine.
L-Fructose was prepared in five steps from L-sorbose (1). 1,2-O-Isopropylidene-cr-L-sorbopyranose (2), prepared from 1, was selectively tosylated using phase transfer catalysis to give 1,2-O-isopropylidene-3-O-(p-tolylsulfonyl)-a-L-sorbopyranose (3). Formation of a 3,4-anhydro ring, followed by its