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Rapid Three-Step One-Pot Microwave-Assisted Synthesis of 2,5-Dioxo-1,2,5,6,7,8-hexahydro-3-quinolinecarbonitrile Library

✍ Scribed by Yermolayev, Sergey A.; Gorobets, Nikolay Yu.; Desenko, Sergey M.

Book ID
111957844
Publisher
American Chemical Society
Year
2009
Tongue
English
Weight
69 KB
Volume
11
Category
Article
ISSN
1520-4766

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Investigation of the one-pot synthesis o
Investigation of the one-pot synthesis ofN-(5,6,7,8-tetrahydro-7,7-dimethyl-2,5-dioxo-2H-1-benzopyran-3-yl-2,5-dioxo-2H-1-benzopyran-3-yl)benzamide
✍ Kočevar, Marijan ;Polanc, Slovenko ;Verček, Bojan ;TiΕ‘ler, Miha πŸ“‚ Article πŸ“… 1990 πŸ› John Wiley and Sons 🌐 English βš– 294 KB

## Abstract A detailed investigation of the reaction of hippuric acid (2) with dimedone (1) and triethyl orthoformate or other one‐carbon sources in acetic anhydride yielding the benzopyran derivative 3 and many byproducts is described. An explanation of this complex process, several attempts to op