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Rapid and simple measurement of ATP-sulfurylase activity in crude plant extracts using an ATP meter for bioluminescence determination

✍ Scribed by Daniel Schmutz; Christian Brunold


Publisher
Elsevier Science
Year
1982
Tongue
English
Weight
373 KB
Volume
121
Category
Article
ISSN
0003-2697

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✦ Synopsis


ATP-sulfurylase (EC 2.7.7.4) catalyzes the first step in assimilatory sulfate reduction, forming adenosine 5'-phosphosulfate (APS) and pyrophosphate from ATP and SO:-. The extractable activity of ATP-sulfurylase was determined in crude extracts from Phaseolus vulgaris by measuring the formation of ATP, produced in the reverse reaction from APS and pyrophosphate, using purified luciferase and luciferin in an ATP meter. One determination can be performed per minute. The rates of ATP-sulfurylase activity determined by this method were about 25 times higher than the ones measured in the forward reaction as AP% formed from ATP and '5SOj-.