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Raman spectroscopic study of 3000-year-old human skeletal remains from a sambaqui, Santa Catarina, Brazil

✍ Scribed by H. G. M. Edwards; D. W. Farwell; D. L. A. de Faria; A. M. F. Monteiro; M. C. Afonso; P. De Blasis; S. Eggers


Publisher
John Wiley and Sons
Year
2001
Tongue
English
Weight
365 KB
Volume
32
Category
Article
ISSN
0377-0486

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✦ Synopsis


A Raman spectroscopic study of red-pigmented human bones from a 3000-year-old sambaqui burial was undertaken for the first time. Visible (633 nm) and near-infrared (1064 nm) excitation were used to characterize the pigment and its substrate; the red pigment is haematite, iron(III) oxide, which proved to be of a pure form and for which no previous heat treatment processing had been adopted. There is clear evidence in heavily pigmented areas of a 'limewash' layer which had been applied to the body of the deceased prior to treatment with ochre. Comparisons made with previous Raman studies of archaeological bone from a separate excavation indicate that mineralization of the present specimens is well advanced, with evidence of calcium carbonate incorporation into the hydroxyapatite phosphatic matrix.