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Radioactivity in deuterated compounds

✍ Scribed by Y. Homma; Y. Murase

Book ID: 112707780
Publisher: Springer
Year: 1990
Tongue: English
Weight: 206 KB
Volume: 146
Category: Article
ISSN: 1588-2780
DOI: 10.1007/bf02165222

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## Abstract 3‐Hydroxy‐4‐(hydroxymethyl)‐5‐(hydroxymethyl‐d~2~)‐2‐methylpyridine(pyridoxine‐d~2~) was prepared by reduction of α^4^‐3‐0‐isopropylidene‐5‐pyridoxic acid with lithium aluminum deuteride. Deuterium was inserted in the 2‐methyl group using base catalyzed exchange between deuterium oxide