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Radicals from Aldehydes: A Convergent Access to Dienes and δ-Lactones.

✍ Scribed by Sharanjeet K. Bagal; Lucie Tournier; Samir Z. Zard

Publisher
John Wiley and Sons
Year
2006
Weight
43 KB
Volume
37
Category
Article
ISSN
0931-7597

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A Novel Synthesis of γ,δ-Unsaturated Ald
A Novel Synthesis of γ,δ-Unsaturated Aldehydes from α-Formyl-γ-lactones
✍ Roger L. Snowden; Robert Brauchli; Simon Linder 📂 Article 📅 2011 🏛 John Wiley and Sons 🌐 German ⚖ 211 KB

## Abstract A preparatively useful one‐step transformation of __γ__,__γ__‐disubstituted __α__‐formyl‐__γ__‐lactones into trisubstituted __γ__,__δ__‐unsaturated aldehydes is described, by means of catalytic amounts of either AcOH or AcOEt in the vapor phase over a glass support. A mechanistic ration