Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.004 A Ê R factor = 0.065 wR factor = 0.172 Data-to-parameter ratio = 15.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
rac-Éthyle 7-(4-chlorophényl)-3a-méthyl-3-(4-nitrophényl)-4a,5-diphényl-3a,4a,8,13-tétrahydro-4H-bis[1,2,4-triazolo][4,3-a:3′,4′-d][1,5]benzodiazépine-1-carboxylate
✍ Scribed by Boudina, Aicha ;Baouid, Abdesselam ;Hasnaoui, Aissa ;Aatif, Abdeljalil ;Eddike, Driss ;Tillard, Monique
- Publisher
- International Union of Crystallography
- Year
- 2007
- Tongue
- English
- Weight
- 216 KB
- Volume
- 63
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
rac-E ´thyle 7-(4-chlorophe ´nyl)-3a-me ´thyl-3-(4-nitrophe ´nyl)-4a,5-diphe ´nyl-3a,4a,8,13te ´trahydro-4H-bis[1,2,4-triazolo][4,3-a:3 0 0 0 ,4 0 0 0 -d]-[1,5]benzodiaze ´pine-1-carboxylate
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The X-ray crystallographic study of the title compound, C 24 H 20 ClN 3 OS, clearly demonstrates that 1,3-dipolar cycloaddition occurs at the C N double bond of the 1,5benzodiazepine.
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