Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.004 A Ê R factor = 0.051 wR factor = 0.140 Data-to-parameter ratio = 15.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
r-1,c-2,c-3,t-4,5-Pentachloro-6-phenyltetralin
✍ Scribed by Bruno, Giuseppe ;Panzalorto, Manuela ;Nicoló, Francesco ;Giannetto, Michele
- Book ID
- 104478892
- Publisher
- International Union of Crystallography
- Year
- 2001
- Tongue
- English
- Weight
- 164 KB
- Volume
- 57
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
The crystal and molecular structure of the title compound, C 19 H 20 Cl 2 O 2 , reveals a chair conformation for the pyran ring in which the hydroxyl group is axially oriented. All the other substituents occupy equatorial positions. There are two molecules in the asymmetric unit.
In the title compound, C 19 H 19 Cl 2 N 3 O 2 , the piperidine ring adopts a distorted boat conformation. In the solid state, the molecules exist as O-HÁ Á ÁN-hydrogen-bonded centrosymmetric dimers.
The thiazolidine ring and the two pyrrolidine rings in the title compound, C 20 H 21 ClN 2 O 2 S 2 , adopt twisted conformations. In the crystal structure, the molecules translated by a unit cell along the a axis are linked by intermolecular C-HÁ Á ÁO hydrogen bonds into a chain and inversion-relate