## Abstract Quantitative analyses have been carried out by ^13^C NMR spectroscopy using Fourier transformation. The Overhauser effect, due to the broad band decoupling of protons, has been suppressed using the two existing methods (gated decoupling and paramagnetic species), and results from each a
Quantitative analysis by nuclear magnetic resonance with fourier transformation: I—Proton case
✍ Scribed by B. Thiault; M. Mersseman
- Publisher
- John Wiley and Sons
- Year
- 1975
- Tongue
- English
- Weight
- 364 KB
- Volume
- 7
- Category
- Article
- ISSN
- 0749-1581
No coin nor oath required. For personal study only.
✦ Synopsis
Abstract
For quantitative analysis by NMR spectroscopy with Fourier transform, the usual experimental conditions have to be partly modified. Careful regulation of the delays between the different phases of the process is particularly important. The filters of the spectrometer and the calculations on the free induction decay are important causes of error. Precise results are given.
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