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Quantitation of the Relative Amounts of Anhydrous Carbamazepine (C15H12N2O) and Carbamazepine Dihydrate (C15H12N2O ·2H2O) in a Mixture by Solid-State Nuclear Magnetic Resonance (NMR)

✍ Scribed by Raj Suryanarayanan; Timothy S. Wiedmann

Book ID
110343325
Publisher
Springer US
Year
1990
Tongue
English
Weight
623 KB
Volume
07
Category
Article
ISSN
0724-8741

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## Abstract According to the ^1^H, ^13^C and ^15^N NMR spectroscopic data and DFT calculations, the __E__‐isomer of 1‐vinylpyrrole‐2‐carbaldehyde adopts preferable conformation with the __anti__‐orientation of the vinyl group relative to the carbaldehyde oxime group and with the __syn__‐arrangement