Quantitation of l-glycero-d-manno-heptose and 3-deoxy-d-manno-octulosonic acid in rough core lipopolysaccharides by partition chromatography
β Scribed by Robert C. Seid Jr.; Herman Schneider; Sophia Bondarew; Robert A. Boykins
- Publisher
- Elsevier Science
- Year
- 1982
- Tongue
- English
- Weight
- 473 KB
- Volume
- 124
- Category
- Article
- ISSN
- 0003-2697
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π SIMILAR VOLUMES
A liquid chromatography (1.6 MPa) system for the analysis of 3-deoxy-Dmanmo-Zoctulosonic acid (KDO), N-acetylneuraminic acid (NeuSAc), methyl CYand &glycosides of NeuSAc and KDO, a-heptosyl-(1+5)-KDO, various sialyllactoses, a-KDO-(2+4)-KDO, a-KDO-(2+4)-KDO methyl a-glycoside, &KDO-(2+4)-KDO methyl
The identification of the peracetylated methyl glycosides of 3-deoxy-o-
The reaction of the peracetate methyl esters of N-acetylneuraminic acid (Neu5Ac), 3-deoxyq~glycero-D-galacto-2-nonulosonic acid (Kdn), and 3-deoxy-D-manno-2-octulosonic acid (Kdo) with trimethylsilyl trifluoromethanesulfonate (CF3SO3SiMe 3) has been reinvestigated. We have found that the choice of s