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Quantification of 1,N6-Etheno-2′-deoxyadenosine in human urine by column-switching LC/APCI-MS/MS

✍ Scribed by Peter R Hillestrøm; Anne-Mette Hoberg; Allan Weimann; Henrik E Poulsen


Book ID
113629169
Publisher
Elsevier Science
Year
2004
Tongue
English
Weight
535 KB
Volume
36
Category
Article
ISSN
0891-5849

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✍ Gabriele Zanchetti; Ivan Floris; Alberto Piccinotti; Silvia Tameni; Aldo Poletti 📂 Article 📅 2012 🏛 John Wiley and Sons 🌐 English ⚖ 327 KB

A method for the rapid and robust confirmation of 11‐nor‐∆9‐tetrahydrocannabinol‐9‐carboxylic acid (THCA) in urine involving basic hydrolysis with NaOH and direct injection of the hydrolysate in a column‐switching LC‐MS‐MS system was developed and validated. THCA‐d3 was used as internal standard. De