A gas chromatographic method is described for the quantification of free and total malondialdehyde (MDA) in biological materials. The procedure involves derivatization of the analyte with 2,4,6-trichlorophenylhydrazine, extraction with n-hexane, and separation of the cyclic derivatization product on
โฆ LIBER โฆ
Quality control in the routine analysis of methylmercury in biological and environmental materials using gas chromatography with electron capture detection
โ Scribed by E. Rubi; R. A. Lorenzo; M. C. Casais; R. Cela
- Publisher
- John Wiley and Sons
- Year
- 1994
- Tongue
- English
- Weight
- 632 KB
- Volume
- 8
- Category
- Article
- ISSN
- 0268-2605
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In this paper we report a way to evaluate the removal of volatile halogenated hydrocarbons formed after break-point chlorination in the Arno river raw water at the Mantignano Utility, Florence, Italy, following dechlorination by hydrogen peroxide. The removal evaluation is performed by GC-ECD on fus