𝔖 Bobbio Scriptorium
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PyBOP®: A new peptide coupling reagent devoid of toxic by-product

✍ Scribed by J. Coste; D. Le-Nguyen; B. Castro

Book ID
104226482
Publisher
Elsevier Science
Year
1990
Tongue
French
Weight
284 KB
Volume
31
Category
Article
ISSN
0040-4039

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An efficient scalable synthesis of 2-halothiazolium-type peptide coupling reagents has been developed. The key step is the formation of the 2-bromothiazole scaffold through cyclization of a-thiocyanato ketones with hydrogen bromide. Using this method, the new coupling reagent 2-bromo-N-methylthiazol