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Pulsed field gradient one-dimensional NMR selective ROE and TOCSY experiments

✍ Scribed by Claudio Dalvit; Günter Bovermann

Publisher
John Wiley and Sons
Year
1995
Tongue
English
Weight
312 KB
Volume
33
Category
Article
ISSN
0749-1581

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✦ Synopsis

Abstract

A pulsed field gradient one‐dimensional NMR selective ROE (rotating frame NOE) experiment was designed and successfully tested. The resulting spectra are of high quality and devoid of artefacts. Hence reliable quantification of very weak ROEs necessary for the three‐dimensional structure determination of a molecule is now possible. A similar experiment was designed for the selective 1D TOCSY pulse sequence.

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