Pulsed field gradient NMR imaging of solids
β Scribed by J.B. Miller; D.G. Cory; A.N. Garroway
- Publisher
- Elsevier Science
- Year
- 1989
- Tongue
- English
- Weight
- 384 KB
- Volume
- 164
- Category
- Article
- ISSN
- 0009-2614
No coin nor oath required. For personal study only.
β¦ Synopsis
The use of multiple pulse line narrowing for NMR imaging of solids is hampered because large magnetic field gradients can place some spins sufficiently far from resonance so that the local line narrowing effkiency is reduced. We propose that this interference can be modeled as a phase error of the rfpulses and can be reduced by appiying the gradient only during selected windows in the pulse cycle. We demonstrate this interference with the use of a digital phase and compare one-dimensional images obtained with the standard static gradient technique and this new pulse gradient method.
π SIMILAR VOLUMES
We present a pulse sequence that enables the accurate and spatially resolved measurements of the displacements of spins in a variety of (biological) systems. The pulse sequence combines pulsed field gradient (PFG) NMR with turbo spin-echo (TSE) imaging. It is shown here that by ensuring that the pha
Β¨ABSTRACT: NMR imaging has been shown to be a viable and useful approach to exploring spatial chemistry and molecular dynamics of a wide range of materials. NMR provides image contrast which is fundamentally different from that of other methods. The principles of NMR imaging and spatial information
The utility of gradient selection in MAS spectroscopy of dipolar solids is explored in two examples. In the first, rotor-synchronized gradients of appropriate strength and duration are applied to select 1H double-quantum coherences. The resulting DQ MAS spectrum of adamantane is compared with that a