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Pulsed EPR and ENDOR investigation of hydrogen atoms in silsesquioxane cages

✍ Scribed by N. Weiden; M. Päch; K. P. Dinse

Book ID
105719555
Publisher
Springer Vienna
Year
2001
Tongue
English
Weight
484 KB
Volume
21
Category
Article
ISSN
0937-9347

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The syntheses of tert-butylgalvinol with perdeuteriated tert-butyl groups and of 1,4-bicyclo[2.2.2]octanebisgalvinol are described. The EPR and ENDOR spectra of the corresponding galvinoxyl monoradicals reveal selective line broadening due to dynamic processes associated with hindered internal rotat