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Préparation, identification et radiocristallographie du sulfite et du pyrosulfite de thallium I anhydres

✍ Scribed by Oddon, Y. ;Tranquard, A. ;Caranoni, C.


Book ID
114498200
Publisher
International Union of Crystallography
Year
1974
Tongue
English
Weight
263 KB
Volume
7
Category
Article
ISSN
0021-8898

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✍ Emile Cherbuliez; Br. Baehler; A. R. Sussmann; J. Rabinowitz 📂 Article 📅 1960 🏛 John Wiley and Sons 🌐 German ⚖ 275 KB 👁 1 views

## Abstract The synthesis of 1‐fluoro‐4,4‐di‐hydroxymethyl‐pentane (I) and its dicarbamate (II) is described. (I) is obtained by classical alkylation of methylmalonic ester with 1‐ bromo‐3‐fluoro‐propane and subsequent reduction with LiAlH~4~, of the fluorinated diester obtained. Treated with phosg