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Production of Bis(trifluoromethyl)benzene

โœ Scribed by Murray, R.; Beanblossom, W.; Wojcik, B.

Book ID
127117489
Publisher
American Chemical Society
Year
1947
Weight
447 KB
Volume
39
Category
Article
ISSN
0019-7866

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1,3-Bis(trifluoromethyl)benzene was regioselectively metalated and subsequently carboxylated at position 2 to give 2,6-bis(trifluoromethyl)benzoic acid. Treatment of the acid with sulphur tetrafluoride gave 2,6-bis-(trifluoromethyl)benzoyl fluoride which was readily converted to 2,6-bis(trifluoromet