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Production of 1-azafluorene from 2-methyl-3-phenylpyridine

✍ Scribed by N. S. Prostakov; A. T. Soldatenkov; V. O. Fedorov

Book ID: 112351321
Publisher: Springer US
Year: 1979
Tongue: English
Weight: 272 KB
Volume: 15
Category: Article
ISSN: 0009-3122
DOI: 10.1007/bf00509801

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THE preparation of 3-methyl-1,2-indandione (I) was first investigated by von Braun and Kirschbaum', who obtained it as a viscous red oil by treatment of 3-methyl-1,2-indandione 2-oxime (II) with aqueous formaldehyde and hydrochloric acid. Shortly thereafter, Steinkopf and Bessaritsck reported the fo