Presentation of sideband envelopes by two-dimensional one-pulse (TOP) spectroscopy
✍ Scribed by B. Blümich; P. Blümler; J. Jansen
- Book ID
- 103963674
- Publisher
- Elsevier Science
- Year
- 1992
- Tongue
- English
- Weight
- 243 KB
- Volume
- 1
- Category
- Article
- ISSN
- 0926-2040
No coin nor oath required. For personal study only.
✦ Synopsis
A novel way of representing 1D MAS spinning sideband spectra in a 2D-resolved fashion is explained. The method is illustrated with 2H MAS data of deuterated polycarbonate. From the resulting 2D spectrum, the isotropic shifts can be identified on one axis and the rotary echo decay spectra along the other axis.
📜 SIMILAR VOLUMES
Poly(vinyl acetate) (PVA) prepared by photopolymerization was studied by a combination of one and two dimensional NMR spectroscopy. The 13 C{ 1 H} and 1 H NMR spectra of the homopolymer (PVA) were assigned to the configurational pentads (CH region) and tetrads (CH 2 region). These assignments were s