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Preparative and structural studies of triphenylphosphonium salts

✍ Scribed by Masood Khan; Colin Oldham; Michael J. Taylor; Dennis G. Tuck

Book ID
103107946
Publisher
Elsevier Science
Year
1980
Weight
241 KB
Volume
16
Category
Article
ISSN
0020-1650

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✍ Qinyan Zhu; Kelley L. Ford; Eric J. Roskamp 📂 Article 📅 1992 🏛 John Wiley and Sons 🌐 English ⚖ 297 KB 👁 1 views

## Abstract Triphenylphosphonium trichlorogermanate was prepared in quantitative yield by reducing germanium tetrachloride‐triphenylphosphine (1:1) with tributyl‐tin hydride in diethyl ether. Heating the phosphonium salt at 245°C gave Ph~3~P‐GeCl~2~ in 90% recrystallized yield. Treatment of the pho