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Preparative and spectroscopic studies of [TlCl3Br(Py)2]−, [TlCl3Br(An)2]−, [TlCl3Br(Qu)2]−, [TlCl3Br(pic3)2]−, [TlCl4(Qu)2]− and [TlCl4]− ions

✍ Scribed by D.N. Sotiropoulos; J.K. Kouinis; A.G. Galinos

Publisher
Elsevier Science
Year
1981
Weight
171 KB
Volume
17
Category
Article
ISSN
0020-1650

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Synthesis and structural characterizatio
Synthesis and structural characterization of a face-sharing bioctahedral complex [HB(Me2Pz)3)BH][Br3Mo(μ-Br)3MoTp*] and an edge-sharing tetramolybdenum complex [Mo4(μ3-O)2(μ2-O)2(μ2-OH)2(O)4(Me2PzH)6](Br)4(Me2PzH2)2 (Tp*=hydridotris(3,5-dimethylpyrazolyl)borate); Pz=pyrazolyl)
✍ Chen-Long Lee; Pang-Yen Yang; Chang-Wei Su; Jhy-Der Chen; Lin-Shu Liou; Ju-Chun 📂 Article 📅 2001 🏛 Elsevier Science 🌐 English ⚖ 151 KB

From a solution prepared by a reaction of Mo 2 (O 2 CCH 3 ) 4 with KTp\* (Tp\*= hydridotris(3,5-dimethylpyrazolyl)borate, HB(Me 2 Pz) 3 ), in diglyme at room temperature followed by addition of excess (CH 3 ) 3 SiBr to the red solution in refluxing THF, the complexes [HB(Me 2 Pz) 3 )BH][Br 3 Mo(m-Br