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Preparative and 1H NMR Investigation on Regioselective Silylation of Starch Dissolved in Dimethyl Sulfoxide

✍ Scribed by Lars Einfeldt; Katrin Petzold; Wolfgang Günther; Armin Stein; Manfred Kussler; Dieter Klemm

Publisher
John Wiley and Sons
Year
2001
Tongue
English
Weight
138 KB
Volume
1
Category
Article
ISSN
1616-5187

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Assessment of the Extent of Starch Disso
Assessment of the Extent of Starch Dissolution in Dimethyl Sulfoxide by 1H NMR Spectroscopy
✍ Sarah Schmitz; Anthony C. Dona; Patrice Castignolles; Robert G. Gilbert; Mariann 📂 Article 📅 2009 🏛 John Wiley and Sons 🌐 English ⚖ 281 KB

## Abstract Complete dissolution is needed for the separation, characterization, or homogeneous labeling of whole starch molecules. A method is presented to quantify the extent of starch dissolution in DMSO for the first time; it is validated on a commercial rice starch. It is used directly on star