𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Preparation of substituted 4-(3-methyl-3-hydroxy-1-butynyl)-2-ethoxy-1,3-dioxolanes

✍ Scribed by I. Yu. Kibina; Sh. M. Musantaeva; A. V. Shchelkunov

Publisher
Springer US
Year
1987
Tongue
English
Weight
138 KB
Volume
23
Category
Article
ISSN
0009-3122

No coin nor oath required. For personal study only.

✦ Synopsis

UDC 547.426'729.7.04 A method has been developed for the preparation of 4-(3-hydroxy-l-alkynyl)-substituted 2-ethoxy-l,3-dioxolanes (which are novel flotation reagents for coal) based on the reaction between acetylene 1,2,5-triols and orthoformic ester in the presence of catalytic quantities of benzoic acid.

📜 SIMILAR VOLUMES

Preparation of 2-Ethoxy-3-hydroxy-4-(per
Preparation of 2-Ethoxy-3-hydroxy-4-(perfluoroalkyl)tetrahydropyran Derivatives from Substituted 4-Ethoxybut-3-en-1-ols
✍ Stig Valdersnes; Leiv K. Sydnes 📂 Article 📅 2009 🏛 John Wiley and Sons 🌐 English ⚖ 356 KB

## Abstract A number of 1‐substituted and 1,1‐disubstituted (__E__)‐4,5,5‐triethoxypent‐3‐en‐1‐ols (**1**) have been converted to perfluoroalkylated tetrahydrofurans and tetrahydropyrans in a selective fashion by 1‐iodoperfluoroalkane addition under radical conditions using sodium dithionite (Na~2~

3-Ethoxy­carbonyl-4-hydroxy-6-(methoxy­m
3-Ethoxy­carbonyl-4-hydroxy-6-(methoxy­methoxy)-1-methyl-2-quinolone
✍ Pozzi, C. Gustavo ;Goeta, Andrés E. ;Autino, Juan C. ;Punte, Graciela 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 269 KB

Single-crystal X-ray study T = 100 K Mean '(C±C) = 0.002 A Ê R factor = 0.041 wR factor = 0.116 Data-to-parameter ratio = 14.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.