## Abstract A method for preparation of mercuri‐derivatives of fluorescein labelled by ^197^Hg or ^203^Hg from mercuric acetate and fluorescein has been described. Individual products formed in the reaction mixture were isolated with both paper chromatography and chromatography on alumina column. T
Preparation of some mercuri-derivatives of fluorescein labelled with isotopes 197Hg and 203Hg. III. Recoil-labelling of derivatives
✍ Scribed by L. Kronrád; J. Ratuský; P. Málek; B. Vavrejn; J. Kolc
- Publisher
- John Wiley and Sons
- Year
- 1970
- Tongue
- French
- Weight
- 300 KB
- Volume
- 6
- Category
- Article
- ISSN
- 0022-2135
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✦ Synopsis
Abstract
The possibility of preparation of mercuriderivatives of fluorescein labelled with ^197^ Hg by irradiation of the respective compounds in a nuclear reactor has been studied. For all investigated compounds, specific activity high enough could be obtained without any significant radiation decomposition. In cases, when the target molecule contained more than one target atom‐bis (hydroxymercurifluoresceinyl) mercury and bis (hydroxymercurifluorescein)‐higher enrichment factor for some products could be obtained. The recommended procedure for preparation of difluoresceinylmercury‐^197^ Hg by this method has been given.
📜 SIMILAR VOLUMES
## Abstract The work is a continuation of the preceding study of possibilities for preparation of labelled derivatives of fluorescein. The conditions under which it is possible to get maximum possible yield of individual products from reaction mixture of mercuric acetate‐^203^Hg and fluorescein has