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Preparation of [I3Cl2]+[SbCl6]- and its characterization by x-ray crystallography and Raman spectroscopy

✍ Scribed by Birchall, Thomas.; Myers, Ronald D.

Book ID
127147739
Publisher
American Chemical Society
Year
1982
Tongue
English
Weight
613 KB
Volume
21
Category
Article
ISSN
0020-1669

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✍ M. S. Arias-Pérez; A. Cosme; E. Gálvez; F. Florencio; I. Fonseca; J. Sanz 📂 Article 📅 1991 🏛 John Wiley and Sons 🌐 English ⚖ 671 KB

## Abstract A series of (±)‐3‐aryl‐1‐azabicyclo[2.2.2]octan‐3‐ols were synthesized and studied by ^1^H, ^13^C and 2D NMR spectroscopy, and the crystal structure of (±)‐3‐(4‐methylphenyl)‐1‐azabicyclo[2.2.2]octan‐3‐ol was determined by X‐ray diffraction. The combined use of COSY, NOESY and ^1^H–^13^