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Preparation of homochiral 9-anthryl-tert-butylcarbinol. The configurational and conformational NMR study of its carbamate derivatives

✍ Scribed by Maria de Moragas; Adriana Port; Xavier Sánchez-Ruiz; Carlos Jaime; Christian Roussel; Albert Virgili

Book ID
103977168
Publisher
Elsevier Science
Year
1995
Tongue
English
Weight
269 KB
Volume
6
Category
Article
ISSN
0957-4166

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✍ Marta Pomares; Xavier Grabuleda; Carlos Jaime; Albert Virgili; Ángel Álvarez-Lar 📂 Article 📅 1999 🏛 John Wiley and Sons 🌐 English ⚖ 101 KB 👁 1 views

2,2-Dimethyl-1-(1-naphthyl)propanol was synthesized and the corresponding enantiomers were isolated by chiral HPLC. These enantiomers gave diastereoisomeric carbamates by reaction with (S)-( )-1-phenylethylisocyanate, which were studied by NMR. The comparison of NMR data and molecular mechanics calc