✦ LIBER ✦
Preparation of formaldehyde by photochemical condensation of carbon monoxide and tritiated hydrogen, and the synthesis of a tritiated morphine derivative
✍ Scribed by A. C. Lane; A. McCoubrey; R. Peaker
- Publisher
- John Wiley and Sons
- Year
- 1966
- Tongue
- French
- Weight
- 254 KB
- Volume
- 2
- Category
- Article
- ISSN
- 0022-2135
No coin nor oath required. For personal study only.
✦ Synopsis
Tritiated formaldehyde, required jor labelling 6:ICendo-etheno-7-(2-hydroxy-2-butyl)-tetrahydro-oripavine (M99), was prepared by photochemical condensation of carbon monoxide and tritiated hydrogen. The specijic activity of the M99 (48 C/mmole) was about one half that of the source of isotope. The loss was traced to undefined secondary decompositions during the photochemical reaction.