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Preparation of Elemental Carbon-13 in High Yield from C 13 O 2

✍ Scribed by Rutherford, William M.

Book ID
126427558
Publisher
American Chemical Society
Year
1966
Tongue
English
Weight
253 KB
Volume
88
Category
Article
ISSN
0002-7863

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A high yield synthesis of 13C- and 14C-l
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✍ William R. Porter; Larry A. Spitznagle; William F. Trager πŸ“‚ Article πŸ“… 1976 πŸ› John Wiley and Sons 🌐 French βš– 255 KB πŸ‘ 1 views

## Abstract Labeled silver carbonate was prepared from barium carbonate‐^13^C or ‐^14^C and aqueous silver nitrate in 95 to 100% yield. Diethyl carbonate‐^13^C or ‐^14^C was generated in 60 to 85% overall yield by treatment of labeled silver carbonate with ethyl iodide and tetraethylammonium iodide