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Preparation of (E)-α,β-unsaturated aromatic aldehydes by high stereoselective olefinformylation.

✍ Scribed by Marcel Gaudemar; Moncef Bellassoued

Publisher
Elsevier Science
Year
1990
Tongue
French
Weight
189 KB
Volume
31
Category
Article
ISSN
0040-4039

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Reduction of Cp2TiC12 with s-BuMgCl in THF gave a greenish deep brown solution which has been found to promote the reductive homocoupling of aromatic and a+-unsaturated aldehydes to yield symmetrical 1,2-diols with high threo-selectivity. threo-1,2-Diols have, after resolution, frequently been utili