Preparation of deuteriated succinic acid
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Masashi Tashiro; Hirohisa Tsuzuki; Shin-Ichiro Isobe; Hideyuki Goto; Shoji Ogasa
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Article
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1991
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John Wiley and Sons
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French
β 361 KB
## Abstract Succinic [2,3β^2^H~2~]β and [2,2,3,3β^2^H~4~]βacids were prepared from maleic anhydride and dimethyl fumarate, and acetylene dicarboxylic acid and its dimethyl ester by treatment with CuAl and NiβAl alloys in 10% NaODβD~2~O in 95% to 100% isotopic purity. The succinic ^2^H~4~ acid havin