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Preparation of Chiral Nitroxide Radicals and Spontaneous Optical Resolution by Recrystallization

✍ Scribed by Dr. Rui Tamura; Shinsuke Susuki; Dr. Nagao Azuma; Prof. Akira Matsumoto; Prof. Fumio Toda; Dr. Akio Kamimura; Dr. Kenzi Hori

Book ID
101556062
Publisher
John Wiley and Sons
Year
1994
Tongue
English
Weight
255 KB
Volume
33
Category
Article
ISSN
0044-8249

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Synthesis, Resolution and Crystal Struct
Synthesis, Resolution and Crystal Structure of a New Optically Active Nitroxide Radical
✍ Benfaremo, Nicholas ;Steenbock, Marco ;Klapper, Markus ;MΓΌllen, Klaus ;Enkelmann πŸ“‚ Article πŸ“… 2006 πŸ› John Wiley and Sons 🌐 English βš– 269 KB

## Abstract The synthesis of the readily available racemate of the nitroxide radical 5 is described. The product exhibits exclusively the __trans__ configuration. The __cis__ product was not obtained. Optically pure enantiomers of 5 were isolated in gram quantities by chiral HPLC. Thus, separation