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Preparation of a 4-monoketal of juglone methyl ether

✍ Scribed by David J. Crouse; Desmond M.S. Wheeler

Book ID: 104238049
Publisher: Elsevier Science
Year: 1979
Tongue: French
Weight: 88 KB
Volume: 20
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(01)86714-9

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✦ Synopsis

Oxidation of 5-methoxy-1-naphthol with thallium trinitrate in ethylene glycol/ trimethylorthoformate gives the 4-ethylene ketal of juglone methyl ether. Monoketals of e-quinones, which have been used as important intermediates in several syntheses', are' made by the selective hydrolysis of the corresponding bisketals (produced

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