✦ LIBER ✦

Preparation of 2 : 4-dinitrobenzenesulphonyl chloride

✍ Scribed by Lunt, E.

Book ID: 102329272
Publisher: Wiley (John Wiley & Sons)
Year: 2007
Weight: 144 KB
Volume: 7
Category: Article
ISSN: 0021-8871
DOI: 10.1002/jctb.5010070806

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✦ Synopsis

4 : 2'-Dihydroxy-2 : 5'-dimethyldiphenylmethane (XIII) .-This compound was synthesized as above from 6-chloro-4-methylol-m-cresol and 9-cresol, and the intermediate chlorodicresylmethane was reduced, without purification, with Raney alloy. Recrystallization of the final product from benzene afforded the dicresylmethane, m.p.

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