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Preparation of 14C- and 18O-enriched allyl alcohol (propanol free)

✍ Scribed by Lidai Kupczyk-Subotkowska; Henry J. Shine

Publisher: John Wiley and Sons
Year: 1992
Tongue: French
Weight: 213 KB
Volume: 31
Category: Article
ISSN: 0022-2135
DOI: 10.1002/jlcr.2580310507

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✦ Synopsis

Abstract

Preparations of specifically labeled [1‐^14^C]‐, [3‐^14^C]‐ and [1‐^18^O]allyl alcohol are described. The syntheses were achieved, respectively, in 7, 11 and 9 steps, with overall yields of 33%, 10% and 38%.

Commercially available K^14^CN, CH~3~^14^COONa and H~2~^18^O were used as the starting materials.

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