Preparation of 1-(4-nitrophenyl)-2-formylpyrrole from furfural
✍ Scribed by É. Baum; T. E. Goldovskaya; V. G. Kul'nevich; O. V. Maiorova
- Book ID
- 112346263
- Publisher
- Springer US
- Year
- 1981
- Tongue
- English
- Weight
- 429 KB
- Volume
- 17
- Category
- Article
- ISSN
- 0009-3122
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📜 SIMILAR VOLUMES
In the title compound, C~14~H~12~N~2~O~3~, the dihedral angle between the two aromatic rings is 86.13 (15)°. Intermolecular N—H...O hydrogen bonds [N...O = 2.886 (3) Å and N—H...O = 174 (3)°] between the NH~2~ and C=O groups link the molecules into a one-dimensional ribbon augmented by secondary N—H
Single-crystal X-ray study T = 295 K Mean (C-C) = 0.004 A R factor = 0.048 wR factor = 0.123 Data-to-parameter ratio = 12.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.