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Preparation, characterization and crystal structure of Fe((OPPh2)2N)3

✍ Scribed by C. Scott Browning; David H. Farrar; Daniel C. Frankel


Publisher
Elsevier Science
Year
1996
Tongue
English
Weight
423 KB
Volume
241
Category
Article
ISSN
0020-1693

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## Abstract BuSnCl~2~[(OPPh~2~)(SPPh~2~)N] (1) and BuSnCl[(OPPh~2~)(SPPh~2~)N]~2~ (2) were prepared by reacting BuSnCl~3~ and K[(OPPh~2~)(SPPh~2~)N], in 1:1 and 1:2 molar ratios. The compounds were investigated in solution by multinuclear (^1^H, ^13^C, ^31^P, ^119^Sn) NMR spectroscopy. Variable‐tem