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Preparation and thermal decomposition reaction kinetics of a dysprosium(III) p-chlorobenzoate 1,10-phenanthroline complex

✍ Scribed by Jian Jun Zhang; Su Ling Xu; Ning Ren; Hai Yan Zhang; Liang Tian

Publisher
John Wiley and Sons
Year
2007
Tongue
English
Weight
189 KB
Volume
40
Category
Article
ISSN
0538-8066

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✦ Synopsis

Abstract

The title complex [Dy(p‐ClBA)~3~Phen]~2~·2H~2~O was synthesized, where p‐ClBA is p‐chlorobenzoate and Phen is 1,10‐phenanthroline. The complex was characterized by various techniques including elemental analysis, IR, XRD, and molar conductance. The thermal decomposition of the complex was studied under the nonisothermal condition by TG‐DTG and IR techniques. The kinetic parameters of dehydration process were obtained from the analysis of DSC curves of the complex by the NL‐DIF and Popescu methods, respectively. © 2007 Wiley Periodicals, Inc. 40: 66–72, 2008

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## Abstract The complex [Sm(__p__‐MBA)~3~phen]~2~ (__p__‐MBA, __p__‐methylbenzoate; phen, 1,10‐phenanthroline) was prepared and characterized by elemental analysis, IR and UV spectra. The thermal decomposition process of [Sm(__p__‐ MBA)~3~phen]~2~ was studied under a static air atmosphere by TG‐DTG