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Preparation and rearrangement of dialkyl and diaryl 1-methyl-1-(trichloromethyl)propyl phosphites

✍ Scribed by V. N. Eliseenkov; V. K. Khairullin

Book ID
112419948
Publisher
Springer
Year
1965
Tongue
English
Weight
327 KB
Volume
14
Category
Article
ISSN
1573-9171

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## Abstract A new and facile method of synthesis of 1‐acetoxyvinyl phosphonates (__2__) has been found. Dialkyl phosphites react readily with acetic anhydride in acetonitrile solution in the presence of catalysts to produce __2__ and acylphosphonates (__1__) as a minor product. The most efficient c