p-[32.56]Octahedrane, the (CH)12 Hydroca
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Dr. Chih-Hung Lee; Dipl.-Chem. Shelue Liang; Dipl.-Chem. Thomas Haumann; Priv.-D
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Article
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1993
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John Wiley and Sons
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English
β 397 KB
and the solution applied to a column (2.5 g, 10 mL) of Bio-Gel P-2(F j from Bio-Rad equilibrated with water. The crude product was purified by HPLC (Gen Pak-Fax column from Waters: A = 0.025 M Tris . HCI, pH 8.5; B = A + 1 M NaCI: linear gradient: 10 to 90% B over 45 min: flow rate = 0.7 mL min-' ;