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Preparation and reactions of perfluoro-.beta.-oxa-.delta.-valerolactone

✍ Scribed by Throckmorton, James R.

Book ID
125497648
Publisher
American Chemical Society
Year
1969
Tongue
English
Weight
427 KB
Volume
34
Category
Article
ISSN
0022-3263

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## Abstract Low‐temperature lithium–iodine exchange between tert‐butyllithium and the appropriate iodide has been used to generate 3‐oxa‐5‐hexenyllithium and a variety of 4‐oxa‐5‐hexenyllithiums. The 3‐oxa system is inherently unstable and fragments via facile β‐elimination to give the anion of all