✦ LIBER ✦

Preparation and Novel Coordination Structure of [Cu(sacch)2(H2O)2] · 4 H2O

✍ Scribed by Professor Li Jianmin; Zhou Yuhong; Zhou Gentao; Wang Quanming; Huang Qun; Wu Xintao

Publisher: John Wiley and Sons
Year: 1996
Tongue: English
Weight: 321 KB
Volume: 31
Category: Article
ISSN: 0232-1300
DOI: 10.1002/crat.2170310213

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✦ Synopsis

Preparation and Novel Coordination Structure of [Cu(sacch)2(H20)2] -4 Ha0 The new cornplex of copper (11) and saccharin -[Cu(sacch)z(HzO)z] . 4 HzO (1) has becri prepared and determined by single crystal X-ray diffraction method. It differs from [Cu(sacch)2(H20)4] . 2 H20 (2) which was reported by HAIDER et al. (1981). The compound (1) crystallizes in the monoclinic space group P21/a with lattice parameters a = 7.326(3) A, b = 16.308(5) b, c = 8.379(1) A, p = 101.09(2)", 2 = 2. Copper(I1) exists in a square planar structure with a CZ axis and rentrosymmetry belonging to the C21, group.

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