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Preparation and Growth Mechanism of Niobium Oxide Microcones by the Anodization Method

✍ Scribed by Zhao, Jianling; Wang, Xixin; Xu, Rongqing; Mi, Yingjuan; Li, Yangxian

Book ID
118017573
Publisher
The Electrochemical Society
Year
2007
Tongue
English
Weight
436 KB
Volume
10
Category
Article
ISSN
1099-0062

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Porous anodic niobium oxide with a pore size of $10 nm was formed at 10 V in glycerol electrolyte containing 0.6 mol dm Γ€3 K 2 HPO 4 and 0.2 mol dm Γ€3 K 3 PO 4 at 433 K. After prolonged anodizing for 5.4 ks, niobium oxide microcones develop on the surface. X-ray diffraction patterns of the anodized