Preparation and evaluation of lauryl methacrylate monoliths with embedded silver nanoparticles for capillary electrochromatography
✍ Scribed by Navarro-Pascual-Ahuir, Maria; Lerma-García, Maria J.; Ramis-Ramos, Guillermo; Simó-Alfonso, Ernesto F.; Herrero-Martínez, José M.
- Book ID
- 119946304
- Publisher
- John Wiley and Sons
- Year
- 2013
- Tongue
- English
- Weight
- 972 KB
- Volume
- 34
- Category
- Article
- ISSN
- 0173-0835
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A novel silica monolithic stationary phase functionalized with octadecanethiol gold nanoparticles (GNPs) was prepared for capillary electrochromatography (CEC). The bare silica monolith was prepared by a sol-gel process and then modified chemically with 3-mercaptopropyltrimethoxysilane, followed by
## Abstract Monolithic columns of capillary electrochromatography (CEC) with weak electroosmotic flow (EOF) have been prepared by in situ polymerization of butyl methacrylate and ethylene dimethacrylate, without any charged groups in the reaction mixture. The reproducibility of such columns has bee