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Preparation and Crystal Structures of ­Purine 2,2′-, 6,6′-, and 8,8′-Dimers

✍ Scribed by Tomáš Tobrman; Petr Štěpnička; Ivana Císařová; Dalimil Dvořák

Publisher
John Wiley and Sons
Year
2008
Tongue
English
Weight
693 KB
Volume
2008
Category
Article
ISSN
1434-193X

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## Abstract Biphenyl‐2,2′,3,3′,5,5′,6,6′‐^2^H~8~ was prepared from biphenyl‐d~10~. Initial bromination of biphenyl‐d~10~ followed by hydrogenolysis of the 4,4′‐dibromobiphenyl‐d~8~ with lithium aluminum hydride gave the desired product in 40% overall yield.