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Preparation and Crystal Structure of Na7Ba14CaN6: A New Subnitride in the NaxBa14CaN6 Series

✍ Scribed by Grigori V. Vajenine; Arndt Simon

Publisher: John Wiley and Sons
Year: 2001
Tongue: English
Weight: 358 KB
Volume: 2001
Category: Article
ISSN: 1434-1948
DOI: 10.1002/1099-0682(200105)2001:5<1189::aid-ejic1189>3.0.co;2-j

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✦ Synopsis

The crystal structure of a new subnitride, Na 7 Ba 14 CaN 6 , could be solved and refined based on single crystal and powder X-ray diffraction data. The compound contains Ba 14 CaN 6 clusters, which are arranged in a Na matrix as in the other subnitrides of the Na x Ba 14 CaN 6 (x = 8, 14, 17, 21, 22) series. The Ba 14 CaN 6 clusters form a slightly distorted ccp arrange- [a]

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