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Preparation and chromatographic characteristics of calix[4]arene polysiloxane as stationary phases for capillary gas chromatography

✍ Scribed by X. H. Lai; L. Lin; C. Y. Wu

Publisher
Springer
Year
1999
Tongue
English
Weight
34 KB
Volume
50
Category
Article
ISSN
0009-5893

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A method for reproducible preparation of
A method for reproducible preparation of chiral polysiloxanes with regular repeat units as stationary phases for capillary gas chromatography
✍ Abe, Iwao ;Nishiyama, Takako ;Frank, Hartmut 📂 Article 📅 1994 🏛 John Wiley and Sons 🌐 English ⚖ 540 KB

## Abstract Trifluoroethyl ester‐functionalized polysiloxanes can be prepared by block condensation of 3‐dichloromethylsilyl‐2‐methylpropionic acid 2′,2′,2′‐trifluoroethyl ester with 1,5‐bis(diethylamino)hexamethyltrisiloxane or with disodium tetramethyldisiloxane‐1,3‐diolate. The functionalized po