## Abstract The preparation of complex ^99m^TcN–MIBI was carried out using two alternative procedures that led to the formation of the complex with high radiochemical purity (>90%). The partition coefficient, electrophoresis and cationic resin exchange experiments showed that the ^99m^TcN–MIBI is a
Preparation and characterization of technetium-99m complexes with new diphosphines containing polyether groups
✍ Scribed by Esteve Valls; David Martin; Carlos Piera; Joan Suades
- Publisher
- John Wiley and Sons
- Year
- 2005
- Tongue
- French
- Weight
- 159 KB
- Volume
- 48
- Category
- Article
- ISSN
- 0022-2135
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A series of reactions between the technetium tricarbonyl core, [^99m^Tc(CO)~3~(OH~2~)~3~]^+^ and both the bifunctional chelate dithiazole valeric acid (DTV) and insulin derivatized with DTV were performed using microfluidic, microwave, and conventional labeling methods. At low concentrations of liga
## Abstract The reactions of V^V^O(O‐__i__Pr)~3~ with [PS3′]H~3~ and [PS3]H~3~ {[PS3′]H~3~ = P(C~6~H~3~‐5‐Me‐2‐SH)~3~, [PS3]H~3~ = P(C~6~H~4~‐2‐SH)~3~} led to the formation of [V^IV^(L)] [L = P2S4′ (1a), P2S4 (1b)], where L was formed by the oxidative coupling of two PS3′ or PS3 ligands by a disulf